HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butyn-1-ol → HCID 86757738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butyn-1-ol | HCID 12991 | — |
| Reactant | HCID 86757739 | HCID 86757739 | — |
| Product | HCID 86757738 | HCID 86757738 | 74% |
Reaction Steps
Ethyl {[4-(2-butynyloxy)phenyl]sulfanyl}[4-(2-thienyl)phenyl]acetate was prepared according to the general method as outlined in example 83 (step 2), starting from ethyl [(4-hydroxyphenyl)sulfanyl][4-(2-thienyl)phenyl]acetate (1.6 g, 4.3 mmol) and 2-butyn-1-ol (0.33 ml, 4.32 mmol); 1.34 g yellow oil. Yield 74%; MS(EI): 421.71 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06340691B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-37acf32e086b404fb79f2ee3d970e526 |
| Source note | uspto-grants-2002_01 |