HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Methyl-3-thiophenecarboxylate chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methylthiophene-3-carboxylic acid | HCID 4625409 | — |
| Product | 2-Methyl-3-thiophenecarboxylate chloride | HCID 22503470 | — |
Reaction Steps
2-Methyl-3-thiophenecarboxylic acid (54 g) was reacted with thionyl chloride (100 ml) at 60° C. for 1.5 hr. The reaction solution was evaporated, and to the resulting residue was added THF (100 ml×2), and then excess thionyl chloride was removed, to give 60.5 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06340759B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-3cd658c25ea145a9ad3206bdedce722e |
| Source note | uspto-grants-2002_01 |