HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18323649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-fluoro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 11053072 | — |
| Reactant | HCID 18323643 | HCID 18323643 | — |
| Product | HCID 18323649 | HCID 18323649 | 69.7% |
Reaction Steps
Following the same procedure reported in the Step 2 of EXAMPLE 13, the reaction of 1-(2-methoxyphenyl)-4-(5-bromovaleryl)piperazine (9.29 mmol) with 6-fluoro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole (3.54 mmol) and triethylamine (4.63 mmol) gave the alkylation product (1.21 g, 53%). mp: 78-81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06342498B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-4c321ff11ffa4c8faa0bf54503113be4 |
| Source note | uspto-grants-2002_01 |