HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1251368Generated: November 3, 2026
Acetone Cyanohydrin → HCID 10560421, compound
https://huagongshe.com/reaction/1251368
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetone Cyanohydrin | HCID 6406 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | Tetrahydrothiopyran-4-one | HCID 66173 | — |
| Product | HCID 10560421 | HCID 10560421 | — |
Reaction Steps
Magnesium sulphate (9.3 g, 77.4 mmoles), DMA (2.25 g, 25.8 mmoles), piperidine (4.4 g, 51.6 mmoles), tetrahydro-4H-thiopyran-4-one (3 g, 25.8 mmoles) and acetone cyanhydrin (2.2 g, 25.8 mmoles) are introduced in succession into a 250 ml two-necked flask. The reaction medium is agitated for 48 hours at 45° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06342511B1 |
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| Source dataset | uspto-grants-2002_01 |
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| ORD ID | ord-6d03aaa6c62443eaa0f43000c4f8de59 |
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| Source note | uspto-grants-2002_01 |
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