HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1,3,5-Triazine, 2,4-dimethoxy-6-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 1,3,5-Triazin-2-amine, 4-methoxy-N,6-dimethyl- | HCID 160779 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | 1,3,5-Triazine, 2,4-dimethoxy-6-methyl- | HCID 19904 | — |
Reaction Steps
Provided herein is a novel and useful process for preparing 2-methoxy-4-methyl-6-methylamino-1,3,5-triazine that broadly comprises the steps of (a) reacting zinc bis(imino-bis-carbimic acid methyl ester) with acetic anhydride to give 2,4-dimethoxy-6-methyl-1,3,5-triazine and (b) reacting the 2,4-dimethoxy-6-methyl-1,3,5-triazine, formed in step (a), with methylamine to give 2-methoxy-4-methyl-6-methylamino-1,3,5-triazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06342600B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-5c425e43e976467d81309fbf85bff1dd |
| Source note | uspto-grants-2002_01 |