HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Triphenylphosphoranylidene)acetaldehyde → HCID 54042463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Triphenylphosphoranylidene)acetaldehyde | HCID 75051 | — |
| Reactant | N-(4-Formyl-1,3-thiazol-2-YL)acetamide | HCID 14931749 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 54042463 | HCID 54042463 | 64.8% |
Reaction Steps
A mixtuxe of 2-acetylamino-4-formylthiazole (6.05 g), formylmethylidenetriphenylphosphorane (10.82 g) and chloroform (360 ml) was refluxed for 4 hours. The precipitates were collected by filtration and washed with chloroform to give 2-acetylamino-4-(2-formylvinyl)thiazole (4.52 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04742057 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-205a10bdd6cd4bc59f2e55e7716fc15f |
| Source note | uspto-grants-1988_05 |