HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14004003, compound → HCID 14004009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14004003 | HCID 14004003 | — |
| Solvent | Borane | HCID 6331 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14004009 | HCID 14004009 | — |
Reaction Steps
To a slightly turbid solution of 3.88 g of 1,4-dihydro-9-methoxybenzo[c]-1,5-naphthyridin-2(3H)-one in tetrahydrofuran (800 ml), 70 ml of borane (0.98M in tetrahydrofuran) was added over approximately one minute. A precipitate formed almost immediately. The suspension was stirred overnight at ambient temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04742061 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-cdc5a3ec550948039d121a34fc5167e6 |
| Source note | uspto-grants-1988_05 |