HRID1252231

反应详情

EQUATION

反应方程式

HRID 1252231 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3-(4-t-butyloxycarbonylphenyl)acrylic acid ethyl ester (11.52 g) and 5% palladium-charcoal in ethanol (115 ml) was stirred under hydrogen atmosphere at room temperature. The catalyst was removed by filtration and washed with ethanol. The combined solution was evaporated to give 3-(4-tert-butyloxycarbonylphenyl)propionic acid ethyl ester.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. washwashed with ethanol
  3. customThe combined solution was evaporated