huagongshe.com
HRID1252346

反应详情

EQUATION

反应方程式

HRID 1252346 的结构方程式

REACTANTS

反应物

2
结构：CC(Br)C(=O)Cl
HCID97980

2-Bromopropanoyl chloride

C3H4BrClO

结构：CC1(C)Cc2cc(S(N)(=O)=O)ccc2O1
HCID15611039

未命名化合物

PRODUCTS

生成物

1
结构：CC(Br)C(=O)NS(=O)(=O)c1ccc2c(c1)CC(C)(C)O2
HCID15611041

未命名化合物

收率 87.7%

PROCEDURE

实验过程

In a manner similar to Step C of Example 9, the reaction of 4.0 g (0.017 mole) of 5-aminosulfonyl-2,3-dihydro-2,2-dimethylbenzofuran with 7.0 mL (0.069 mole) of 2-bromopropionyl chloride produced 5.4 g of N-(2,3-dihydro-2,2-dimethylbenzofuran-5-yl)sulfonyl-2-bromopropionamide as a solid (mp 125°-128° C.).