HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trimethoxybutane → 5-Methyl-4-imidazolecarboxylic acid, 2-(1-methoxybutylidene)hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trimethoxybutane | HCID 123512 | — |
| Reactant | 5-Methyl-1H-imidazole-4-carbohydrazide | HCID 12953270 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-Methyl-4-imidazolecarboxylic acid, 2-(1-methoxybutylidene)hydrazide | HCID 57304460 | — |
Reaction Steps
A mixture of 10 g of 5-methyl-1H-imidazole-4-carboxylic acid hydrazide, 80 ml of trimethylorthobutyrate and 395 ml of absolute ethanol was treated and described in Example 1, giving 16.5 g of 5-methyl-4-imidazolecarboxylic acid, 2-(1-methoxybutylidene)hydrazide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04743586 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-2d9aeb3eead34b789fd849770c530202 |
| Source note | uspto-grants-1988_05 |