HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → HCID 14255054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | 2-(Pyridin-3-yl)ethan-1-amine | HCID 854051 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14255054 | HCID 14255054 | — |
Reaction Steps
A mixture of 4.89 g of isatoic anhydride, 3.66 g of 2-(3-pyridinyl)ethylamine and 40 ml of ethanol was stirred at room temperature for 22 hours. The reaction mixture was concentrated and the residue was dissolved in ethyl acetate and cooled. The desired product was isolated by filtration, mp 126°-128° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04743610 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-b8aee358253345de95442f3df219b01a |
| Source note | uspto-grants-1988_05 |