Phthalic Anhydride → HCID 14255063, compound

HRID 1252491Notes

Reaction equation

HRID 1252491 reaction equation
[C:1]1(=[O:11])[O:6][C:4](=[O:5])[C:3]2=[CH:7][CH:8]=[CH:9][CH:10]=[C:2]12.[N:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH2:18][CH2:19][NH2:20])[CH:13]=1>C(Cl)Cl>[N:12]1[CH:17]=[CH:16][CH:15]=[C:14]([CH2:18][CH2:19][NH:20][C:4]([C:3]2[CH:7]=[CH:8][CH:9]=[CH:10][C:2]=2[C:1]([OH:6])=[O:11])=[O:5])[CH:13]=1

Participants

4

Reactant 2

HCID 6811Phthalic AnhydrideHCID 8540512-(Pyridin-3-yl)ethan-1-amine

Product 1

HCID 14255063HCID 14255063, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of 4.44 g of phthalic anhydride and 75 ml of methylene chloride was stirred and 3.66 g of 2-(3-pyridinyl)ethylamine was added. Solution occured followed by separation of a white precipitate. The desired product was separated by filtration and melted at 183°-185° C.

Workup

  1. customSolution occured followed by separation of a white precipitate
  2. customThe desired product was separated by filtration and melted at 183°-185° C.

Sources & evidence

ORD record
ord-3bc3e685d25d48d28322e284ef0a4aaf
Source dataset
uspto-grants-1988_05
Patent number
US04743610

Reaction notes

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