HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → HCID 14255063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | 2-(Pyridin-3-yl)ethan-1-amine | HCID 854051 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14255063 | HCID 14255063 | — |
Reaction Steps
A mixture of 4.44 g of phthalic anhydride and 75 ml of methylene chloride was stirred and 3.66 g of 2-(3-pyridinyl)ethylamine was added. Solution occured followed by separation of a white precipitate. The desired product was separated by filtration and melted at 183°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04743610 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-3bc3e685d25d48d28322e284ef0a4aaf |
| Source note | uspto-grants-1988_05 |