HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzoylmethane → HCID 53873802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzoylmethane | HCID 8433 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Cetyl chloroformate | HCID 97633 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 53873802 | HCID 53873802 | — |
Reaction Steps
The preparation is carried out as described in Example 1, using 44.8 g (0.2 mole) of dibenzoyl methane, 61.0 g (0.2 mole) of n-hexadecyl chloroformate and 200 ml of diethyl ether as well as 22 g (0.22 mole) of triethylamine. The resultant yellow viscous liquid crystallises out. The crystals melt at 39°-40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04743640 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-97265bc7686e4009a9f457f5df083cb9 |
| Source note | uspto-grants-1988_05 |