HRID1252516

反应详情

EQUATION

反应方程式

HRID 1252516 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The preparation is carried out as described in Example 1, using 44.8 g (0.2 mole) of dibenzoyl methane, 61.0 g (0.2 mole) of n-hexadecyl chloroformate and 200 ml of diethyl ether as well as 22 g (0.22 mole) of triethylamine. The resultant yellow viscous liquid crystallises out. The crystals melt at 39°-40° C.

WORKUP

后处理

  1. customThe resultant yellow viscous liquid crystallises out
  2. custommelt at 39°-40° C.