HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(5-Bromo-3-methyl-2-pyridinyl)butylamine → HCID 178422460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(5-Bromo-3-methyl-2-pyridinyl)butylamine | HCID 13094272 | — |
| Reactant | HCID 14086552 | HCID 14086552 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178422460 | HCID 178422460 | — |
Reaction Steps
A mixture of 0.514 g (0.0021 mole) of 4-(5-bromo-3-methyl-2-pyridinyl)butylamine and 0.463 g (0.0021 mole) of 3-(methylthio)thieno[2,3-d]isothiazole 1,1-dioxide in 35 ml of ethanol was heated under reflux with stirring for 4 hours. The reaction solution was cooled in ice giving a crystalline product which amounted to 0.71 g, m.p. 191°-193° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04743692 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-5d72514672d84616b01d394895aa8a30 |
| Source note | uspto-grants-1988_05 |