HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 6-Phenyl-5-p-tolyl-pyridine-2-carboxylate → Methyl 6-phenyl-5-(p-tolyl)picolinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 6-Phenyl-5-p-tolyl-pyridine-2-carboxylate | HCID 25033077 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 6-phenyl-5-(p-tolyl)picolinate | HCID 25033163 | — |
Reaction Steps
Following General Procedure E, ethyl 6-phenyl-5-p-tolyl-pyridine-2-carboxylate (Compound 22, 70 mg, 0.22 mmol) and conc. H2SO4 (3 drops) in MeOH (3 ml) were reacted to produce the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728014B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-3bbe9e8d5be141679a7e56b70fc93128 |
| Source note | uspto-grants-2010_06 |