HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-(4-ethylphenyl)-6-phenylpyridine-2-carboxylate → Methyl 5-(4-Ethylphenyl)-6-phenyl-pyridine-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-(4-ethylphenyl)-6-phenylpyridine-2-carboxylate | HCID 25033078 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 5-(4-Ethylphenyl)-6-phenyl-pyridine-2-carboxylate | HCID 25033164 | — |
Reaction Steps
Following General Procedure E, ethyl 5-(4-ethylphenyl)-6-phenylpyridine-2-carboxylate (Compound 23, 45 mg, 0.15 mmol) and conc. H2SO4 (3 drops) in MeOH (3 ml) were reacted to produce title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728014B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-c8f862b8d57b4ed5a6bad16f2966582d |
| Source note | uspto-grants-2010_06 |