2-Chlorobenzaldehyde → HCID 20139029, compound

HRID 1252705Notes

Reaction equation

HRID 1252705 reaction equation

[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[CH2:12][C:13]#[N:14].[Cl:15][C:16]1[CH:23]=[CH:22][CH:21]=[CH:20][C:17]=1[CH:18]=O.C(Cl)(Cl)Cl.C(OCC)(=[O:30])C>>[Br:1][C:2]1[C:11]2[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=2[CH:5]=[C:4]2[C:3]=1[CH2:12][C:13](=[O:30])[NH:14][CH:18]2[C:17]1[CH:20]=[CH:21][CH:22]=[CH:23][C:16]=1[Cl:15]

Participants

4

Reactant 3

HCID 69962-Chlorobenzaldehyde

HCID 2343772-(1-bromonaphthalen-2-yl)acetonitrile

HCID 21584013Chloroform ethylacetate

Product 1

HCID 20139029HCID 20139029, compound

Procedure

This compound was prepared from 1-bromo-2-naphthylacetonitrile and 2-chlorobenzaldehyde. m.p. 256°-257° C. (chloroform-ethyl acetate).

Sources & evidence

ORD record: ord-229765b010f54476b5cadceec13c4cb1
Source dataset: uspto-grants-1988_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04745115

Reaction notes

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