HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxy-3,4-dimethylbenzenemethanol acetate → HCID 20137829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxy-3,4-dimethylbenzenemethanol acetate | HCID 148394 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 20137829 | HCID 20137829 | 4.4% |
Reaction Steps
A solution of intermediate D (5.1 g, 0.21 mole) in 100 ml of methanol and 25 ml of 10% sodium hydroxide was refluxed for one hour, then poured into ice water. The resulting solid was collected by filtration and dried to give 1.8 g of 1,4-dimethoxy-2,3-dimethyl-5-hydroxymethylbenzene (intermediate E).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746607 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-fc5c1a741d4d42a6bf9eabfb14273127 |
| Source note | uspto-grants-1988_05 |