HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20137892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20137881 | HCID 20137881 | — |
| Product | HCID 20137892 | HCID 20137892 | — |
Reaction Steps
A mixture of 377 mg of methyl 4-(α-phosphonoacetamido)-picolinate and 4.2 ml of 1N sodium hydroxide is heated at 80° for 10 minutes. The reaction mixture is cooled, filtered through Dowex 50-X8 resin and evaporated to dryness. Trituration with ethanol affords 4-(α-phosphonoacetamido)-picolinic acid, m.p. 249°-252° (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746653 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-6167c1a3d402492bb166fbd25ffcdb80 |
| Source note | uspto-grants-1988_05 |