Ethyl 5-(4-ethylphenyl)-3-methyl-6-phenylpyridine-2-carboxylate → HCID 59338841, compound

HRID 12531Notes

Reaction equation

HRID 12531 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:10]=[C:11]([CH3:26])[C:12]([C:21]([O:23][CH2:24]C)=[O:22])=[N:13][C:14]=2[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:5][CH:4]=1)[CH3:2]>OS(O)(=O)=O.CO>[CH2:1]([C:3]1[CH:4]=[CH:5][C:6]([C:9]2[CH:10]=[C:11]([CH3:26])[C:12]([C:21]([O:23][CH3:24])=[O:22])=[N:13][C:14]=2[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:7][CH:8]=1)[CH3:2]

Participants

4

Reactant 1

HCID 68408281Ethyl 5-(4-ethylphenyl)-3-methyl-6-phenylpyridine-2-carboxylate2×

Product 1

HCID 59338841HCID 59338841, compound

Reagents, catalysts & solvents 2

HCID 1118Sulfuric AcidCatalystHCID 887MethanolSolvent

Procedure

Following General Procedure E, ethyl 5-(4-ethylphenyl)-3-methyl-6-phenylpyridine-2-carboxylate (Compound 26, 29 mg, 0.08 mmol) and conc. H2SO4 (3 drops) in MeOH (5 ml) were reacted to produce the title compound as an oil.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-ad10b7d5192549c796b757eb7bdd7792
Source dataset
uspto-grants-2010_06
Patent number
US07728014B2

Reaction notes

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