HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetohydrazide → HCID 178485101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetohydrazide | HCID 14039 | — |
| Reactant | HCID 20137152 | HCID 20137152 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178485101 | HCID 178485101 | — |
Reaction Steps
Methyl 5-[4-[2-methylguanidino)-1,2,3-triazol2-yl]valerimidate (1.0 g.) in MeOH (12 ml.) was treated with acethydrazide (0.22 g.) and the solution stirred for 18 nours. Evaporation of the solvent and trituration of the resioue with ether/EtOH gave N-acetylamino-5[4-(2-methylguanidino)-1,2,3-triazol-2-yl]valeramidine as a yellow sticky solid [0.54 g.) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04748165 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-ad5cbedd866444acaf8289d46b677549 |
| Source note | uspto-grants-1988_05 |