HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanate → HCID 53787466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Reactant | HCID 20137164 | HCID 20137164 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53787466 | HCID 53787466 | — |
Reaction Steps
A solution of 5-(4-amino-1,2,3-triazol-2-yl)valeronitrile (1.65 g.) in acetonitrile (6 ml.) was treated with ethylisothiocyanate (0.87 g.) and the solution stirred for 2.5 days then heated under reflux for 4.5 hours. Evaporation of the solvent gave 5-[4-(3-ethylthioureido)-1,2,3-triazol-2-yl]valeronitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04748165 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-e82122b92bd14f68a638e6154bfec3c9 |
| Source note | uspto-grants-1988_05 |