Diflunisal → HCID 70413194, compound

Participants

Reaction Conditions

Reaction Steps

83 grams of diflunisal, dissolved in 500 ml ethanol, were added to an aqueous solution of 65 g meglumine, by stirring slowly and at room temperature (20° C.), and the reaction mixture was maintained under stirring for 4 hours until the reaction was complete. After cooling at 7° C., the resulting white precipitate was filtered and washed with small quantities of ethanol. After drying, 139 g of diflunisal meglumine were obtained as a white microcrystalline powder.

Provenance & Evidence