HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Aminobenzo[d]thiazol-6-yl)methanol → 2-Aminobenzo[d]thiazole-6-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Aminobenzo[d]thiazol-6-yl)methanol | HCID 13821540 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Aminobenzo[d]thiazole-6-carbaldehyde | HCID 13821541 | — |
Reaction Steps
110.5 g (0.613 mol) of 1a are stirred in 200 ml of THF with 319.8 g (3.678 mol) of manganese (IV) oxide at room temperature for 3 days. The reaction mixture is filtered, the residue on the filter is washed with THF, and the filtrate is evaporated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04748163 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-ca3210786c364083880abbc75021adba |
| Source note | uspto-grants-1988_05 |