反应详情

110.5 g (0.613 mol) of 1a are stirred in 200 ml of THF with 319.8 g (3.678 mol) of manganese (IV) oxide at room temperature for 3 days. The reaction mixture is filtered, the residue on the filter is washed with THF, and the filtrate is evaporated in vacuo.

1. filtrationThe reaction mixture is filtered
2. washthe residue on the filter is washed with THF
3. customthe filtrate is evaporated in vacuo