HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 54538331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Bromo-1,1,2-trifluorobut-1-ene | HCID 66333 | — |
| Reactant | 4,5-Dimethyloxazol-2-amine | HCID 535870 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 54538331 | HCID 54538331 | 34.7% |
Reaction Steps
In a manner similar to Example 9, Step (a), 2-amino-4,5-dimethyloxazole (3.0 grams, 0.027 mole), carbon disulfide (2.67 grams, 0.035 mole), triethylamine (3.44 grams, 0.34 mole), dimethyl sulfoxide (13.5 ml) and 4-bromo-1,1,2-trifluoro-1-butene (6.43 grams, 0.034 mole) were reacted to produce 2.78 grams of (3,4,4-trifluoro-3-butenyl) N-(4,5-dimethyl-2-oxazolyl)dithiocarbamate. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04748186 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-cd235d75e5e440ca88643a9253793fbb |
| Source note | uspto-grants-1988_05 |