Dimethylformamide dimethyl acetal → HCID 21807119, compound

Participants

Reaction Conditions

Reaction Steps

To N,N-dimethylformamide dimethyl acetal (0.384 ml, 2.88 mmol) was added methyl-3-oxo-pentanoate (250 mg, 1.92 mmol) and the mixture was heated to 110° C. in a sealed vessel. After 30 minutes the reaction mixture was cooled and concentrated to afford methyl (2Z)-2-[(dimethylamino)methylene]-3-oxopentanoate which was used without further purification.

Provenance & Evidence