HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxy-1,8-naphthyridine-2,6-dicarboxylic acid → HCID 178516463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxy-1,8-naphthyridine-2,6-dicarboxylic acid | HCID 178524139 | — |
| Solvent | Quinoline | HCID 7047 | — |
| Product | HCID 178516463 | HCID 178516463 | — |
Reaction Steps
To quinoline (500 ml) was added 5-hydroxy-1,8-naphthyridine-2,6-dicarboxylic acid (50 g, 340 mmol). The reaction mixture was heated to reflux. After 8 hours, the reaction mixture was cooled and concentrated in vacuo to afford 1,8-naphthyridin-4-ol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08455477B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-a4f02701fbec4e1494183cd36e7ee939 |
| Source note | uspto-grants-2013_06 |