HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → HCID 71294308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | 5-Cyclohexyl-6-(2,2,2-trifluoro-ethoxy)-pyridin-3-ylamine | HCID 71294148 | — |
| Product | HCID 71294308 | HCID 71294308 | 48.1% |
Reaction Steps
This compound was prepared following the same procedure as described for Example 3 using 5-cyclohexyl-6-(2,2,2-trifluoro-ethoxy)-pyridin-3-ylamine (Example 8b) (100 mg, 0.36 mmol) and benzoic acid (40 mg, 0.33 mmol) as starting materials. The title compound (60 mg, 43.5%) was isolated as off white solid; MS (ESI): 379 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08455501B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-5884380a090542f3ae3aac25e183d3d9 |
| Source note | uspto-grants-2013_06 |