N-Iodosuccinimide → HCID 178433059, compound

Participants

Reaction Conditions

Reaction Steps

To the product of Step 2 (750 mg, 3.2 mmol) in 10 mL of CFI3CN was added N-iodosuccinimide (710 mg, 3.2 mmol). The mixture was stirred at 25° C. for 1 h, cooled to −20° C. The precipitate was collected by filtration, washed with cold Et2O and dried to give 4-iodo-2-methyl-5-[4-(methylsulfonyl)phenyl]-1H-imidazole. LCMS: [M+1]+=362.9.

Provenance & Evidence