Phenylphosphonic Acid → HCID 68627267, compound

HRID 1255391Notes

Reaction equation

HRID 1255391 reaction equation
[C:1]1([P:7](=[O:10])([OH:9])[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.O.O.O.O.O.S([O-])([O-])(=O)=O.[Cu+2:21]>O>[C:1]1([P:7](=[O:8])([O-:10])[O-:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cu+2:21]

Participants

4

Reactant 2

HCID 15295Phenylphosphonic AcidHCID 24463Copper sulfate pentahydrate

Product 1

HCID 68627267HCID 68627267, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

130 parts of phenylphosphonic acid was dissolved in 1350 parts of water. To the resulting solution was added 103 parts of copper sulfate pentahydrate, and the resulting mixture was stirred for two hours at room temperature. The precipitate was filtered, washed with water, and then dried under reduced pressure at 100° C., yielding 35 parts of copper phenylphosphonate.

Workup

  1. filtrationThe precipitate was filtered
  2. washwashed with water
  3. customdried under reduced pressure at 100° C.

Sources & evidence

ORD record
ord-06056945589a45e68a5b1e641ab8d195
Source dataset
uspto-grants-2013_06
Patent number
US08461075B2

Reaction notes

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