HuagongsheHuagongshe Chemistry Print Report · For research reference only
Furan → HCID 13904348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Furan | HCID 8029 | — |
| Reactant | Tetrachlorocyclopropene | HCID 80428 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13904348 | HCID 13904348 | — |
Reaction Steps
A stirred mixture of 1,2,3,3-tetrachlorocyclopropene (60 g) and furan (22.97 g) in dry toluene (600 ml) was heated to reflux for 30 hours. The solvent was evaporated under reduced pressure to afford the required product, 75.4 g. 1H NMR (CDCl3) δ: 6.90 (1H, dd), 6.45 (1H, dd), 5.41 (1H, d), 4.93 (1H, d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461083B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-6c8324c40aa7422f9f894984aa04e7f4 |
| Source note | uspto-grants-2013_06 |