HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 66969198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 86651352 | HCID 86651352 | — |
| Product | HCID 66969198 | HCID 66969198 | 94% |
Reaction Steps
The title compound was prepared in a similar manner as Example 13 Step 1, utilizing methyl (1R,10E, and 10Z,14S,18R,22S,25S)-22-cyclopentyl-7,20,23-trioxo-2,19-dioxa-8,21,24-triazatetracyclo[22.2.1.03,8.014,18]heptacosa-3,5,10-triene-25-carboxylate and replacing THF with ethanol as the solvent to give a 94% yield. LCMS (ES+) m/z 544.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461107B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-e558c31c6ff94d4799482014b6d38d2f |
| Source note | uspto-grants-2013_06 |