HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloropyridine-2-carboxylic acid → HCID 49820224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloropyridine-2-carboxylic acid | HCID 230890 | — |
| Reactant | HCID 57496586 | HCID 57496586 | — |
| Product | HCID 49820224 | HCID 49820224 | — |
Reaction Steps
The coupling of [(S)-4-(3-amino-phenyl)-1,4-dimethyl-6-oxo-1,4,5,6-tetrahydro-pyrimidin-2-yl]-carbamic acid tert-butyl ester from experiment F1 and 4-chloro-pyridine-2-carboxylic acid followed by deprotection of the intermediate yielded the title compound as a colourless solid. MS (ESI): m/z=372.1 [ M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461160B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-5d2eb893718b41dd832c85308b2f6a19 |
| Source note | uspto-grants-2013_06 |