HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 1-(5,6-Diphenyl-pyridin-2-yl)-propan-1-one Oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | 1-(5,6-Diphenyl-pyridin-2-yl)-propan-1-one | HCID 25033167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(5,6-Diphenyl-pyridin-2-yl)-propan-1-one Oxime | HCID 136332339 | — |
Reaction Steps
Following General Procedure P, 1-(5,6-diphenyl-pyridin-2-yl)-propan-1-one (Compound 76, 90 mg, 0.31 mmol), NH2OH—HCl (87 mg, 1.25 mmol) and pyridine (272 mg, 0.27 mmol) in EtOH (2 ml) were reacted to give title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728014B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-de35d10a8fda445dbd46ff8369b0ab92 |
| Source note | uspto-grants-2010_06 |