HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → HCID 11460315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | 1-(Bromomethyl)-4-chlorobenzene | HCID 69329 | — |
| Product | HCID 11460315 | HCID 11460315 | 41.8% |
Reaction Steps
In the same manner as in Example 6 (1), a crude product was obtained using diethyl malonate (13.6 g) and 4-chlorobenzyl bromide (17.5 g). This was purified by silica gel column chromatography to give the title compound (10.1 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461209B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-cdcd98bac78c4c87b4d1c52e95658a85 |
| Source note | uspto-grants-2013_06 |