HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68508069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 86645219 | HCID 86645219 | — |
| Product | HCID 68508069 | HCID 68508069 | — |
Reaction Steps
To the compound (2.10 g) obtained in Example 110 (4) were added 0.5 mol/L hydrochloric acid (40 ml) and ethyl acetate (80 mL), and the organic layer was collected by partitioning and washed with brine. The organic layer was concentrated under reduced pressure to give the title compound (1.90 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461209B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-0c6c56b6d5784a5181f83d5b4ab8d006 |
| Source note | uspto-grants-2013_06 |