HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethylaniline → N-ethyl-N'-(2-naphthylsulfonyl)-N-phenyl-2-(2-propynyl)malonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethylaniline | HCID 7670 | — |
| Reactant | N,N-diethyl-N'-(2-naphthylsulfonyl)-2-(2-propynyl)malonamide | HCID 86645224 | — |
| Product | N-ethyl-N'-(2-naphthylsulfonyl)-N-phenyl-2-(2-propynyl)malonamide | HCID 86645223 | — |
Reaction Steps
In the same manner as in Example 1 (4), a crude product was obtained using the compound (4.00 g) obtained in Example 152 (4) and N-ethylaniline (1.53 mL). This was purified by silica gel column chromatography to give the title compound (98 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461209B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-9a6e884a11a444489a7b55874245379a |
| Source note | uspto-grants-2013_06 |