HRID1257132

反应详情

EQUATION

反应方程式

HRID 1257132 的结构方程式

PROCEDURE

实验过程

The 2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene and NaOH are mixed in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W to perform hydrolysis reaction for no more than 20 minutes to obtain 2,5-dicarboxy-3,4-ethylenedioxythiophene. The reaction is shown in the chemical formula (D).

WORKUP

后处理

  1. temperatureThe microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W
  2. customhydrolysis reaction for no more than 20 minutes