HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → 2,3-Dihydro-thieno(3,4-b)(1,4)dioxin-5,7-dicarboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Diethyl 2,3-dihydrothieno[3,4-b][1,4]dioxine-5,7-dicarboxylate | HCID 625399 | — |
| Produkt | 2,3-Dihydro-thieno(3,4-b)(1,4)dioxin-5,7-dicarboxylic acid | HCID 728841 | — |
Reaktionsschritte
The 2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene and NaOH are mixed in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W to perform hydrolysis reaction for no more than 20 minutes to obtain 2,5-dicarboxy-3,4-ethylenedioxythiophene. The reaction is shown in the chemical formula (D).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08461355B2 |
| Quelldatensatz | uspto-grants-2013_06 |
| ORD ID | ord-e714056c8ea14213a8ec2ddd553539a4 |
| Quellennotiz | uspto-grants-2013_06 |