1,3-Dichloroacetone → HCID 66939077, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 2-fluoro-3-(trifluoromethyl)benzamide (1.02 g), 1,3-dichloropropanone (1.27 g) and toluene (4 mL) was heated at 130° C. for 40 hr. The reaction mixture was purified by column chromatography (carrier: silica gel, eluent: hexane-ethyl acetate) to give the title compound (0.81 g) as colorless crystals.

Provenance & Evidence