HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58127681, compound → HCID 58127974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58127681 | HCID 58127681 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 58127974 | HCID 58127974 | 95% |
Reaction Steps
The compound (0.08 g) obtained in Example 122b was dissolved in ethyl acetate (2 ml), palladium carbon (5 mg) was added, and the mixture was stirred under a hydrogen atmosphere at room temperature overnight. Palladium carbon was removed by filtration, and the solvent was evaporated from the filtrate under reduced pressure to give the title compound (0.06 g) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08461348B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-ee1661a1b76c4c85b97698170ced9361 |
| Source note | uspto-grants-2013_06 |