3,4-Difluorobenzoyl chloride → HCID 11428459, compound

Participants

Reaction Steps

The title compound was prepared in a manner similar to that described in Example 2 by using 5,6-dihydro-4H-thieno[2,3-d]azepine-8-carboxylic acid ethyl ester and 3,4-difluoro-benzoyl chloride. 1H-NMR(CDCl3): δ 8.01 (1 H, s), 7.47 (1 H, m), 7.36 (1H, m), 7.27 (2H, m), 6.85 (1H, d), 4.23 (2H, q), 4.13 (2H, m), 3.15 (2H, t), 1.23 (3H, t). MS (ES): 364 (MH+).

Provenance & Evidence