HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 42281543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione | HCID 94834 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 42281543 | HCID 42281543 | — |
Reaction Steps
A mixture of 40% aqueous methylamine (70 mL) and camphoric anhydride (5 g) was stirred at room temperature for 30 minutes. To this N,N-dimethyl-4-aminopyridine (DMAP) (0.67 g, 5.4 mmol) was added and stirred further for 24 hours. The reaction mixture was allowed to cool to room temperature and acidified with con. HCl at 0-5° C. White precipitate formed was filtered and dried (5.2 g). m/z (M+H): 214.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466145B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-1be69acfa2d24dae8fcb58eb7f2d0830 |
| Source note | uspto-grants-2013_06 |