HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1258366Generated: October 28, 2026
Tributylstannane → (E)-3-(tributylstannyl)prop-2-en-1-ol
https://huagongshe.com/reaction/1258366
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tributylstannane | HCID 5948 | — |
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Propargyl alcohol | HCID 7859 | — |
| Product | (E)-3-(tributylstannyl)prop-2-en-1-ol | HCID 10043273 | — |
Reaction Steps
To neat propargyl alcohol (5 ml) were added tributyltin hydride (29.2 ml) followed by AIBN (716 mg). The mixture was heated for 2.75 h at 80° C., cooled to RT and directly purified by CC (EA/Hept 5/95) to afford the desired compound (12.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08466156B2 |
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| Source dataset | uspto-grants-2013_06 |
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| ORD ID | ord-b676fd4be60d4fe29784cb4f17e1530d |
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| Source note | uspto-grants-2013_06 |
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