反应详情

温度

80 °C

To neat propargyl alcohol (5 ml) were added tributyltin hydride (29.2 ml) followed by AIBN (716 mg). The mixture was heated for 2.75 h at 80° C., cooled to RT and directly purified by CC (EA/Hept 5/95) to afford the desired compound (12.9 g).

1. temperaturecooled to RT
2. customdirectly purified by CC (EA/Hept 5/95)