HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58338482, compound → HCID 135862907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58338482 | HCID 58338482 | — |
| Catalyst | Mercuric acetate | HCID 15337 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 135862907 | HCID 135862907 | — |
Reaction Steps
610 mg of 1-(1H-pyrrolo[2,3-b]pyridine-3-carbonyl)-4-phenylthiosemicarbazide and 686 mg of mercury(II) acetate in 6 ml of MeOH are stirred at 80° C. for 2 hours in a sealed screw-lid vial. 1 drop of Na2S solution is added to the cooled reaction solution, everything is filtered through kieselguhr with suction and rinsed with warm MeOH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466170B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-6c726e1ef03249fdb1b7de39bf5d0c9d |
| Source note | uspto-grants-2013_06 |