Triphenylphosphine → HCID 68506593, compound

Participants

Reaction Conditions

Reaction Steps

The mixture of Examples 24i and 24ii was dissolved in a mixed solvent of THF (3 mL) and H2O (0.25 mL). To the mixture, PPh3 (147 mg, 0.56 mmol) was added. The mixture was stirred at 70° C. for 2 h, and then cooled down. The reaction mixture was purified by SCX cartridge to give a mixture of Examples 25i and 25ii.

Provenance & Evidence